Minnesota State University Moorhead
Dr. Craig P. Jasperse, Chemistry
Phone: (218) 477-2230            Home: (218) 291-9841 
Office: Hagen407J              email: jasperse@mnstate.edu           fax: (218) 477-2137
Office Hours:   Mon 12:00-2:00 Tues 1:00-3:00 Wed 12:00-2:00 Thurs 9:00-11:00 Fri 12:00-2:00

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Chem 350
Chem 355
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Chem 210
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Full Chem 355 Syllabus       Required Text and Materials for Fall 2008      Lab Manual
Safety Information     To access safety information, go to the MSUM Chem link, click "resources", and
                        you will get links to three safety lectures and a useful list of Safety-related Acronyms

Chem 355 Lab Schedule Fall 2008     
Week and Date Experiment Expt.# Jasperse Note: Update Links below
1 Aug 25-27 Checkin, Melting Points Melting Range Handout
2 Sept 2-3 Molecular Structure Molecular Modelling Handout
3 Sept 8-10 Solubility Tests; Crystallization of Phtallic Acid Recrystallizaton-1 Handout
4 Sept 15-17 Recrystallization of Acetanilide Using Mixed Solvent; Recrystallization of an Unknown Recrystallization-2 Handout
5 Sept 22-24 Simple and Fractional Distillation of a Mixture Distillation Handout
6 Sept 29-Oct 1 Liquid/liquid Extraction; Extraction of Acids and Bases Acid-Base Extraction Handout
7 Oct. 8-11 Nucleophilic Substitution of Alkyl Halides
Mechanisms and Arrow Pushing 		SN2-SN1 Handout
Oct 13-15 No Lab. Fall breather, Registration Advising.  
8 Oct 20-22 Nuclear Magnetic Resonance Spectroscopy;
Determination of an Unknown by 13C NMR 		C-13 NMR Handout
NMR User's Guide
C13-NMR Interpretation (Condensed)
9 Oct 27-Oct 29 Thin-Layer Chromatography; Column Chromatography Chromatography Handout
10 Nov. 3-5 1H NMR Determination of an Unknown H-NMR Handout
H-NMR Interpretation (Condensed)
11 Nov 10-12 Grignard Synthesis of Triphenylmethanol Grignard Handout
Standard Synthesis Report Format
12 Nov 17-19 Grignard Synthesis Continued  
13 Dec 1-3 Sodium Borohydride Reduction of 2-Methylcyclohexanone. Use of 1H NMR to measure product ratios. Cleanup, Checkout Borohydride Handout