Minnesota State University Moorhead
Dr. Craig P. Jasperse, Chemistry
Phone: (218) 477-2230            Home: (218) 291-9841 
Office: Hagen407J              email: jasperse@mnstate.edu           fax: (218) 477-2137
Office Hours:   Mon-Wed-Fri 12-2 Tues 1-3 Thurs 9-11

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Chem 350
Chem 355
Chem 360
Chem 365
Chem 210
Chem 341
Chem 342
Chem 150
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Full Lab Manual for Printing
Full Chem 355 Syllabus       Required Text and Materials for Fall 2009      
Safety Information     To access safety information, go to the MSUM Chem link, click "resources", and
                        you will get links to three safety lectures and a useful list of Safety-related Acronyms

Chem 355 Lab Schedule Fall 2008     
Week and Date Experiment Expt.# Jasperse Note: Update Links below
1 Aug 24-26 Checkin, Melting Points Melting Range Handout
2 Aug 31-Sept 2 Solubility Tests; Crystallization of Phtallic Acid
 Recrystallizaton-1 Handout
3 Sept 8-9 Molecular Structure Molecular Modelling Handout
4 Sept 14-16 Recrystallization of Acetanilide Using Mixed Solvent; Recrystallization of an Unknown Recrystallization-2 Handout
5 Sept 21-23 Simple and Fractional Distillation of a Mixture Distillation Handout
6 Sept 28-30 Liquid/liquid Extraction; Extraction of Acids and Bases Acid-Base Extraction Handout
7 Oct. 5-7 Nucleophilic Substitution of Alkyl Halides
Mechanisms and Arrow Pushing 		SN2-SN1 Handout
Oct 12-14 No Lab. Fall breather, Registration Advising.  
8 Oct 19-21 Nuclear Magnetic Resonance Spectroscopy;
Determination of an Unknown by 13C NMR 		C-13 NMR Handout
NMR User's Guide
C13-NMR Interpretation (Condensed)
9 Oct 26-Oct 28 Thin-Layer Chromatography; Column Chromatography Chromatography Handout
10 Nov. 2-4 1H NMR Determination of an Unknown H-NMR Handout
H-NMR Interpretation (Condensed)
11 Nov 9-11 Grignard Synthesis of Triphenylmethanol Grignard Handout
Standard Synthesis Report Format
12 Nov 16-18 Grignard Synthesis Continued  
13 Nov 30 - Dec 2 Sodium Borohydride Reduction of 2-Methylcyclohexanone. Use of 1H NMR to measure product ratios. Cleanup, Checkout Borohydride Handout